2,8,14,20-Tetra-kis(4-hydroxy-phen-yl)-pyrogallol[4]arene dimethyl-formamide hexa-solvate

Eric E. Dueno; Thomas Ray; Ralph N. Salvatore; Cesar Zambrano; Matthias Zeller; Allen D. Hunter

doi:10.1107/S1600536807021071

2,8,14,20-Tetra-kis(4-hydroxy-phen-yl)-pyrogallol[4]arene dimethyl-formamide hexa-solvate

Eric E. Dueno^*
, Thomas Ray
, Ralph N. Salvatore
, Cesar Zambrano
, Matthias Zeller
, Allen D. Hunter

^*Corresponding author for this work

Eastern Kentucky University
Lehman College
Youngstown State University

Research output: Contribution to journal › Article › peer-review

2 Scopus citations

Abstract

The title compound, C52H40O16·6C3H7NO, is shown to adopt a macrocyclic chair conformation. The asymmetric unit contains one-half of the main mol-ecule, which lies on a crystallographic inversion center, together with three solvent molecules. Extensive inter-molecular O - H⋯O hydrogen bonding between the hydroxyl groups and dimethyl-formamide mol-ecules generates a three-dimensional network.

Original language	English
Pages (from-to)	o3533-o3534
Journal	Acta Crystallographica Section E: Structure Reports Online
Volume	63
Issue number	8
DOIs	https://doi.org/10.1107/S1600536807021071
State	Published - 31 Jul 2007

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title = "2,8,14,20-Tetra-kis(4-hydroxy-phen-yl)-pyrogallol[4]arene dimethyl-formamide hexa-solvate",

abstract = "The title compound, C52H40O16·6C3H7NO, is shown to adopt a macrocyclic chair conformation. The asymmetric unit contains one-half of the main mol-ecule, which lies on a crystallographic inversion center, together with three solvent molecules. Extensive inter-molecular O - H⋯O hydrogen bonding between the hydroxyl groups and dimethyl-formamide mol-ecules generates a three-dimensional network.",

author = "Dueno, \{Eric E.\} and Thomas Ray and Salvatore, \{Ralph N.\} and Cesar Zambrano and Matthias Zeller and Hunter, \{Allen D.\}",

year = "2007",

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doi = "10.1107/S1600536807021071",

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T1 - 2,8,14,20-Tetra-kis(4-hydroxy-phen-yl)-pyrogallol[4]arene dimethyl-formamide hexa-solvate

AU - Dueno, Eric E.

AU - Ray, Thomas

AU - Salvatore, Ralph N.

AU - Zambrano, Cesar

AU - Zeller, Matthias

AU - Hunter, Allen D.

PY - 2007/7/31

Y1 - 2007/7/31

N2 - The title compound, C52H40O16·6C3H7NO, is shown to adopt a macrocyclic chair conformation. The asymmetric unit contains one-half of the main mol-ecule, which lies on a crystallographic inversion center, together with three solvent molecules. Extensive inter-molecular O - H⋯O hydrogen bonding between the hydroxyl groups and dimethyl-formamide mol-ecules generates a three-dimensional network.

AB - The title compound, C52H40O16·6C3H7NO, is shown to adopt a macrocyclic chair conformation. The asymmetric unit contains one-half of the main mol-ecule, which lies on a crystallographic inversion center, together with three solvent molecules. Extensive inter-molecular O - H⋯O hydrogen bonding between the hydroxyl groups and dimethyl-formamide mol-ecules generates a three-dimensional network.

UR - https://www.scopus.com/pages/publications/34547734479

U2 - 10.1107/S1600536807021071

DO - 10.1107/S1600536807021071

M3 - Artículo

AN - SCOPUS:34547734479

SN - 1600-5368

VL - 63

SP - o3533-o3534

JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

IS - 8

ER -

2,8,14,20-Tetra-kis(4-hydroxy-phen-yl)-pyrogallol[4]arene dimethyl-formamide hexa-solvate

Abstract

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