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Dispersion of graphene in ethanol by sonication

  • M. Cayambe
  • , C. Zambrano
  • , T. Tene
  • , M. Guevara
  • , G. Tubon Usca
  • , H. Brito
  • , R. Molina
  • , D. Coello-Fiallos
  • , L. S. Caputi
  • , C. Vacacela Gomez
  • GraphenTech NL
  • Universidad Técnica Particular de Loja
  • Escuela Superior Politécnica de Chimborazo
  • Universidad Técnica de Ambato
  • University of Calabria
  • Universidad Yachay Tech

Research output: Contribution to journalConference articlepeer-review

25 Scopus citations

Abstract

Graphene is prepared from natural graphite flakes by solvent dispersion and short-sonication time. In this study, we exfoliate few-layer graphene (FLG) directly in ethanol without adding high boiling point solvents, surfactants or polymers. Diverse characterization methods are employed to scrutinize the morphology and quality of the obtained graphene. UV-visible spectrum is characterized by a prominent peak at 269 nm, corresponding to the p to p* transitions of graphene. Raman spectroscopy show that exfoliated FLG to be free of basal-plane defects. Scanning electron microscopy (SEM) evidence semitransparent FLG layers. Transmission electron microscopy (TEM) presents folded (or folded edge) graphene sheets. As the sonication time is reduced, the proposed method shows a great promise for the industrial-scale synthesis of graphene for many applications, from high-frequency electronics to smart coatings.

Original languageEnglish
Pages (from-to)4027-4030
Number of pages4
JournalMaterials Today: Proceedings
Volume37
DOIs
StatePublished - 2019
Externally publishedYes
Event2019 International Conferences and Exhibition on Nanotechnologies, Organic Electronics and Nanomedicine, NANOTEXNOLOGY 2019 - Thessaloniki, Greece
Duration: 29 Jun 20196 Jul 2019

Keywords

  • Ethanol
  • Few-layer graphene
  • Raman
  • SEM
  • Sonication
  • TEM
  • UV-Visible

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